Please use this identifier to cite or link to this item:
Title: Synthesis and vibrational analysis of some organotin compounds.
Authors: Wycherley, Glenn.
Award date: 1974
Presented at: University of Leicester
Abstract: An investigation was carried out into the formation of alkyl tin compounds from basic, aqueous solutions of tin(II). By varying the composition of the reactants and reaction conditions, the yields of alkyl tin compounds were optimised and mechanisms were postulated for the reactions involved. The Raman spectra of tin(II) solutions were recorded and discussed. The properties of alkyl tin oxides are described, with particular reference to the vibrational spectra of dialkyl tin oxides. The preparations of dialkyl tin dihalides from dialkyl tin oxides are discussed, and an examination made of the infrared and Raman spectra of the products. Single crystal vibrational spectra of dimethyl tin dichloride and dimethyl tin dibromide were recorded and assignments made of the spectra which were obtained.
Level: Doctoral
Qualification: Ph.D.
Rights: Copyright © the author. All rights reserved.
Appears in Collections:Theses, Dept. of Chemistry
Leicester Theses

Files in This Item:
File Description SizeFormat 
U419276.pdf9.68 MBAdobe PDFView/Open

Items in LRA are protected by copyright, with all rights reserved, unless otherwise indicated.